Crystal structure of bis[mu(2)-5,11-bis(diphenylphosphanyl)-25,26-dipropyloxy-27,28-bis(2-pro penyl)calix[4]arene-P:P ']disilver(I) bis(tetrafluoroborate) - dichloromethane (1:2), [Ag-2(C64H62O4P2)(2)][BF4](2)center dot 2CH(2)Cl(2)
Résumé
C65H64AgBCl2F4O4P2, monoclinic, P12(1)/n1 (no 14), a = 16 6993(8) angstrom, b = 23 1203(9) angstrom, c = 17 0133(7) angstrom, beta = 115 197(6)degrees, V = 5943 8 angstrom(3), Z = 4, R-gt(F) = 0.080, wR(ref)(F-2) = 0 215, T = 150 K